Table 4
Precision (Intermediate assay and Intra-day) validation for dieckol in phlorotannin preparations

Concentration (μg/mL)

Instruments

Dieckol content (mg/g)

Average content (mg/g)

SD (mg/g)

RSD (%)

Itermediate assay

94.56231

Agilent 1260

73.930

74.453

0.920

1.236

97.25632

Agilent 1260

75.057

93.42563

Agilent 1260

73.044

98.62358

Agilent 1200

75.384

Phlorotannin sample (mg)

Concentration (μg/mL)

Dieckol content (mg/g)

Average content (mg/g)

SD (mg/g)

RSD (%)

Intra-day: Agilent 1260 Infinitya

56.5

96.10084

74.1592

73.9297

0.761

1.030

59.4

101.08464

74.1968

58.3

97.25135

72.7300

56.6

95.55534

73.6080

57.9

99.64617

75.0358

52.7

89.26187

73.8485